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Efficient reduction of graphene oxide na

Mohamad Fahrul Radzi Hanifah, Juhana Jaafar

2026engraphene oxidereduced graphene oxidesodium oxalatechemical reductionnanomaterialscharacterization

Abstract

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The efficient synthesis of reduced graphene oxide (RGO) nanosheets via a chemical reduction process of exfoliated graphene oxide (GO) nanosheets was performed by introducing sodium oxalate (Na2C2O4) as a reducing agent. This study aimed to investigate the effects of reduction time on the synthesized RGO, with GO being reduced at intervals of 0.5, 1, and 2 hours for RGO-1, RGO-2, and RGO-3, respectively. The carbon/oxygen atomic ratio of the synthesized RGO-3 was found to increase significantly from 2.16 to 6.32 after reduction, as determined by X-ray photoelectron spectroscopy (XPS). Morphological analysis of RGO-3, conducted using high-resolution transmission electron microscopy (HRTEM), revealed the formation of single-layer structures. Moreover, it was observed that the number of RGO layers decreased with increased reduction time. These results indicate that sodium oxalate plays a crucial role in the effective removal of oxygen-containing groups in GO, thus producing high-quality RGO suitable for various applications.

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Cite This Work

@article{533f8762-f6ec-4b89-9bfd-1654728867eb,
  title={Efficient reduction of graphene oxide na},
  author={Mohamad Fahrul Radzi Hanifah and Juhana Jaafar},
  year={2026},
  language={en}
}
TY  - JOUR
TI  - Efficient reduction of graphene oxide na
AU  - Mohamad Fahrul Radzi Hanifah
AU  - Juhana Jaafar
PY  - 2026
LA  - en
ER  -

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