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Synthesize and characterization of graph

Razieh Jabari Seresht, Mohsen Jahanshahi

2026engraphenegraphene oxidenanoporous materialssurface areaexfoliationcharacterization

Abstract

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A few-layer graphene was obtained by the expansion and exfoliation of water-intercalated graphene oxide via heat treatment in nitrogen environment in the temperature range of 200–1000 ◦ C. Graphene which was synthesized at 800 ◦ C (GT800) had a higher quality than other temperatures. This graphene has a high specific surface area (560.6 m 2 g− 1 ) and nano-porous structure. However, as for the purpose of comparison, graphene was synthesized with a colloidal suspension of exfoliated graphene oxide sheets in water with hydrazine hydrate in various reaction times (12, 24 and 36 h). This method has obtained a six-layer graphene and graphene that was synthesized during 24 h reaction with hydrazine hydrate (GC24) had a higher quality in comparison with the other products. The GC24 had 195.97 m 2 g− 1 specific surface area and nano-porous structure. The as-synthesized graphene were then characterized by X-ray diffraction (XRD), Fourier transform infrared (FT-IR) spectroscopy, Raman spectroscopy, transmission electron microscopy (TEM), scanning electron microscopy (SEM) as well as BET measurements. The results demonstrated that this low-cost method for few-layer graphene, e.g. three-layers, fabrication is reliable and promising.

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Cite This Work

@article{7ba62d16-5dc6-45be-bd55-55595ad8d8c9,
  title={Synthesize and characterization of graph},
  author={Razieh Jabari Seresht and Mohsen Jahanshahi},
  year={2026},
  language={en}
}
TY  - JOUR
TI  - Synthesize and characterization of graph
AU  - Razieh Jabari Seresht
AU  - Mohsen Jahanshahi
PY  - 2026
LA  - en
ER  -

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