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Corrosion and protection of lead anodes

L. Cifuentes, E. Astete

2026encorrosionlead anodescopper electrowinningsulphuric acidcurrent interruptions

Abstract

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It is known that lead anodes used in the industrial extraction of copper by electrolysis (electrowinning) suffer corrosion due to current interruptions. This study aims to enhance understanding of the corrosion and protection mechanisms of lead anodes by analyzing the effects of various solute concentrations, including copper, sulphuric acid, cobalt, iron, manganese, chloride, and an organic additive (guar), on lead corrosion. The methodology employs weight loss tests and surface analysis techniques such as X-ray photoelectron spectroscopy, X-ray diffraction, and wavelength dispersive spectroscopy. Results indicate that the corrosion rate of lead during current interruptions increases with the concentration of sulphuric acid and copper, while cobalt, iron, and chloride reduce the corrosion rate. Notably, manganese does not decrease corrosion and precipitates on the lead anode surface under the tested conditions. A method for establishing the optimum anode protection current density during current interruptions is proposed, highlighting three ranges of current densities. The 'high' protection range corresponds to the increased compactness of the PbO2 layer at current densities exceeding 60 A m−2.

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Cite This Work

@article{b45069c8-ab81-4697-9a0c-201a76633ffe,
  title={Corrosion and protection of lead anodes},
  author={L. Cifuentes and E. Astete},
  year={2026},
  language={en}
}
TY  - JOUR
TI  - Corrosion and protection of lead anodes
AU  - L. Cifuentes
AU  - E. Astete
PY  - 2026
LA  - en
ER  -

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