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Recovery of germanium from leach solutio (1)

Hossein Kamran Haghighi, Mehdi Irannajad

2026engermaniumsolvent extractionfly ashAlamine 336Aliquat 336Cyanex 923

Abstract

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The solvent extraction of germanium and some heavy metals by commercial tri-octyl/decyl amine (Alamine 336), N-methyl-N, N-diocyl chloride (Aliquat 336) and phosphine oxide (Cyanex 923) has been studied. In each extraction system, germanium was only extracted from a solution containing nickel, cadmium, cobalt, and zinc, which had a composition similar to gasification coal fly ash aqueous leach solutions. Under comparable conditions, the germanium extraction efficiency by the aforementioned extractants was found to be in the order Aliquat 336>Alamine 336>Cyanex 923. The slope analysis method indicated that 2 moles of Alamine 336 and Aliquat 336, as well as 4 moles of Cyanex 923, participated in the extraction of germanium. Amine extraction systems required tartaric acid as a complexant to convert germanium to anionic species, where a mole ratio of 2 was essential for complete complexation. Moreover, oxalic acid at a concentration of 0.1 M was identified as an effective solvated complexant in the Cyanex 923 system. HCl solutions at 1 and 2 M concentrations effectively stripped germanium from the loaded Alamine 336 and Aliquat 336, respectively, while a 0.1 M NaOH solution sufficed for stripping from Cyanex 923. Consequently, Aliquat 336 emerged as an economical and industry-friendly extractant for germanium solvent extraction from a mixed solution.

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Cite This Work

@article{d45642f5-c45f-4c04-9049-5b9c20aabb02,
  title={Recovery of germanium from leach solutio (1)},
  author={Hossein Kamran Haghighi and Mehdi Irannajad},
  year={2026},
  language={en}
}
TY  - JOUR
TI  - Recovery of germanium from leach solutio (1)
AU  - Hossein Kamran Haghighi
AU  - Mehdi Irannajad
PY  - 2026
LA  - en
ER  -

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